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Preparation and Morphology of Poly(butylene succinate) Nanofibers via Electrospinning

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Abstract:

An electrospinning method was used to produce Poly(butylene succinate) (PBS) nanofibres. The morphology of the fibres was studied considering fibres of different weight concentrations of PBS/CF solution and spun with different diameters of needle-orifice. The results show that the electrospinning process is very difficult and the products are only by few fibres when the weight concentration equals 8%. When the concentration is increased, the eff-iciency is high and the process becomes easy. The morphology of the fibres is more uniform when are spun with a larger diameter of the needle-orifice. The electrospinability ranges between 8 wt% and 14wt% of PBS/CF weight concentration. The thermal properties and the crystallisation of the PBS polymer pellets and electrospun PBS nanofibers were measured by differential scanning calorimetry (DSC) and wide angle X-ray diffraction (WAXD), respectively. In addition, the hydrolytic degradation behaviour of electrospun PBS nanofibres in 1N NaOH solution was observed by using scanning electron microscopy (SEM).

Tags: electrospinning, PBS, nanofibers, morphology, characterization.

Published on issue no 4 (63) / 2007, pages 30–33.

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"Fibres & Textiles in Eastern Europe" is inserted on the "ISI Master Journal List" of the Institute for Scientific Information, Philadelphia, USA (for the year 2010 has an Impact Factor of 0.629) and is indexed in Research Alert, SCI Expanded (Sci Search and Web of Science), the Materials Science Citation Index, Current Contents/Engineering, Computing & Technology; as well as by the Textile Institute, Manchester, in the Information Service; and in Toga FIZ Technik; Rapra Technology Ltd.; Elsevier Geo Abstracts; Textiles Eastern Europe - World Textile Publications; Applied Mechanics Review; Chemical Abstracts Service; Referativny hurnal; and by the European Textile Network.

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